Molecular Formula | C23H43NP2 |
Molar Mass | 395.54 |
Melting Point | 116-119°C |
Boling Point | 456.3±45.0 °C(Predicted) |
Flash Point | 67℃ |
Appearance | Powder |
Color | white to light-yellow |
pKa | 5.72±0.24(Predicted) |
Storage Condition | Keep in dark place,Inert atmosphere,Room temperature |
Sensitive | air sensitive |
Risk Codes | R14/15 - R36/37/38 - Irritating to eyes, respiratory system and skin. |
Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S43 - In case of fire use ... (there follows the type of fire-fighting equipment to be used.) |
UN IDs | UN 2813 4.3 / PGIII |
WGK Germany | 3 |
Introduction | 2, 6-bis (di-tert-butylphosphomethyl) pyridine is an organic intermediate, 6-bis (chloromethyl)-pyridine is obtained by nucleophilic substitution with di-tert-butylphosphine. 2,6 -bis (di-tert-butylphosphomethyl) pyridine can be used to produce high quality and reproducible inorganic films on solid substrates. The film may act as a dielectric, fine-structure separator or as an electrical contact in a transistor, preferably as an electrical contact. |
Use | di-tert-butylphosphine (1.25g,8.6 mmol) was added dropwise to 2, A suspension of 6-bis (chloromethyl)-pyridine (710 mg,4.0 mmol) in methanol (3 mL). The mixture was heated to 45 °c and stirred for 2 days. After cooling to room temperature, triethylamine (1.25mL) was added slowly and a white precipitate formed. The solvent was evaporated in vacuo and the compound 2,6 -bis (di-tert-butylphosphomethyl) pyridine was separated from the residue by column chromatography (silica, solvent: Chloroform), white solid. |